CERTIFICATE OF ANALYSIS QUALITY CONTROL PERFORMANCE REPORT |
COLUMN INFORMATION
SERIAL NUMBER : 2019006133
PART NUMBER : S8034-034360 PRODUCT TYPE : ChraSep SPE Columns ODS-IC 500mg/3ml, 50/pk LOT : 639753201
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HPLC Test Conditions Column Dimension: 100 x 4.6 mm, Flow 1 mL/min Detector UV@254 nm Mobile Phase Methanol:Water (60:40) Temperature 25-35 oC Probes: Uracil, Acetophenone, Nitrobenzene, Benzene, Toluene |
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MATERIAL SAFETY DATA SHEETS ARE AVAILABLE UPON REQUEST |
ChraReport at https://chrareport.com/2019006133 |
RAW MATERIALS
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Properties
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Specifications
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Results
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Methods
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Tube Purity |
Proprietary |
Pass |
GC FID Test |
Frit Purity |
Proprietary |
Pass |
GC FID Test |
Base Silica PhysicalComponent Properties |
Properties
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Specifications
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Results
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Methods
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Specific Surface Area (m2/g) |
450-550 |
535
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N2 BET |
Average Particle Size (µm) |
45-60 |
46 |
Malvern 100 |
Average Pore Diameter (Å) |
60-90 |
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N2 BET |
Particle Size Distribution (%) |
≤20µm ≤ 35µm ≥80µm
≤ 11 ≤18 ≤15
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≤20µm ≤ 35um ≥80um
≤ 8 ≤15 ≤10
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Malvern 100 |
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PRODUCT SPECIFICATION/ANALYSIS
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Bonded Silica Properties: BOND SI 40UM C18 TOLUENCE
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Properties
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Specifications
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Results
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Methods
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Tube Purity
|
Proprietary
|
Pass
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GC FID Test
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Frit Purity
|
Proprietary
|
Pass
|
GC FID Test
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Base Silica Physical Properties
|
Properties
|
Specifications
|
Results
|
Methods
|
Specific Surface Area (m2/g)
|
450-550
|
535
|
N2 BET
|
Average Particle Size (µm)
|
45-60
|
46
|
Malvern 100
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Average Pore Diameter (Å)
|
60-90
|
|
N2 BET
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Particle Size Distribution (%)
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≤20µm ≤ 35µm ≥80µm
≤ 11 ≤18 ≤15
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≤20µm ≤ 35µm ≥80µm
≤ 8 ≤15 ≤10
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Malvern 100
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PRODUCT SPECIFICATION/ANALYSIS
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Bonded Silica Properties: ChraSep SPE Columns ODS-IC 40UM
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Properties
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Specifications
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Results
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Methods
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Carbon Loading (%C)
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17.0-20.0
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19.5
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CHNO-S Analysis
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Hydrogen Loading(%H)
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1.5-6.0
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3.95
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CHNO-S Analysis
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Surface Coverage (µmol/m2)
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1.90-2.50
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2.05
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Calculated based on %C
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Turbidity (NTU)
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≤10.0
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0.55
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Turbidity meter
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Washable Residue (mg/g)
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≤2.0
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0.2
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Methanol and Hexane gravimetric
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Bed Mass Consistency
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Proprietary
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Pass
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Weight Measurement
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Flow Characteristics
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Proprietary
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Pass
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Methanol in low vacuum (1” Hg)
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ChraReport at https://chrareport.com/2019006133 |